146038-45-1Relevant academic research and scientific papers
DIALKYL TRIMETHYLSILYL TETRATHIOPHOSPHATES. SYNTHESIS AND TRANSFORMATIONS
Nizamov, I.S.,Kuznetsov, V.A.,Batyeva, E.S.,Al'fonsov, V.A.
, p. 1196 - 1198 (2007/10/02)
We have developed an efficient method for synthesizing dialkyl trimethylsilyl tetrathiophosphates, which react with aldehydes, acetals, ortho esters, thioacetals, bis(thiocyanato)methane, diethyl disulfide, and alkyl halides to give a number of new tetrathiophosphate derivatives.
CONVENIENT SYNTHESIS OF S-TRIMETHYLSILYL ESTERS OF DITHIO- AND TETRATHIOPHOSPHORIC ACIDS
Nizamov, Il'yas,Kuznetzov, Vladislav A.,Batyeva, Elvira S.,Al'Fonsov, Vladimir A.,Pudovik, Arkady N.
, p. 179 - 186 (2007/10/02)
S-Trimethylsilyl esters of dithio- and tetrathiophosphoric acids were obtained in the reaction of tetraphosphorus decasulfide with alkoxy- and alkylthiotrimethylsilanes, trimethylsilyl enol ethers and bis(trimethylsilyloxy)alkylenes and phenylene. Key words: S-Trimethylsilyl esters of dithio- and tetrathiophosphoric acids; tetraphosphorus decasulfide; alkoxy- and alkylthiotrimethylsilanes; trimethylsilyl enol ethers; bis(trimethylsilyloxy)alkylenes
