14747-97-8Relevant academic research and scientific papers
Synthesis of a tetraazido-substituted 2-tetrazene from 1,5-cyclooctadiene and iodine azide
Rose, Bernd,Schollmeyer, Dieter,Meier, Herbert
, p. 409 - 412 (1997)
In contrast to the addition of iodine azide to cyclooctene (1) or 1,3-cyclooctadiene (5), its reaction with 1,5-cyclooctadiene (12) leads mainly to the surprisingly stable tetraazido-substituted 2-tetrazene 14. The structure of this was established by 15N-NMR studies and an X-ray structural analysis. Treatment of 14 with hydrochloric acid yields the diazido-substituted 9-azabicyclo[3.3.1]nonane 20. VCH Verlagsgesellschafi mbH, 1997.
