Liebigs Annalen p. 409 - 412 (1997)
Update date:2022-08-18
Topics:
Rose, Bernd
Schollmeyer, Dieter
Meier, Herbert
In contrast to the addition of iodine azide to cyclooctene (1) or 1,3-cyclooctadiene (5), its reaction with 1,5-cyclooctadiene (12) leads mainly to the surprisingly stable tetraazido-substituted 2-tetrazene 14. The structure of this was established by 15N-NMR studies and an X-ray structural analysis. Treatment of 14 with hydrochloric acid yields the diazido-substituted 9-azabicyclo[3.3.1]nonane 20. VCH Verlagsgesellschafi mbH, 1997.
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