158519-34-7Relevant articles and documents
Synthesis and conformational analysis of N-glycopeptides that contain extended sugar chains
Urge, Laszlo,Jackson, David C.,Gorbics, Livia,Wroblewski, Krysztof,Graczyk, Graczyna,Otvos Jr., Laszlo
, p. 2373 - 2390 (1994)
Maltooligosaccharides with 2-7 sugar moieties were converted into β-1-amino-1-deoxy derivatives and were coupled to N(α)-fluorenylmethoxycarbonyl-L-aspartic acid α-tert-butyl-β-pentafluorophenyl ester. After trifluoroacetic acid deprotection, the resultin
Solid-phase synthesis of glycopeptides: Synthesis of N(α)-fluorenylmethoxycarbonyl L-asparagine N(β)-glycosides
Urge,Kollat,Hollosi,Laczko,Wroblewski,Thurin,Otvos Jr.
, p. 3445 - 3448 (1991)
It was found that crude 1-glycosylamines, prepared with satured aqueous NH4HCO3 from reducing sugars, can be coupled with Fmoc-Asp(OPfp)-O(t)Bu in N,N-dimethylformamide-water mixtures. Purification and removal of the (t)Bu group resu