16601-28-8Relevant academic research and scientific papers
SYNTHESES OF 2-MERCAPTO- AND 2-ALKYLTHIO-1,3-PROPANEDIOL DERIVATIVES
Aveta, Raffaele,Brandt, Alberto,Corsi, G. Bruno,Costanza, Angela Mitidieri
, p. 649 - 652 (2007/10/02)
Some synthetic routes to 2-alkylthio-1,3-propanediol derivatives, starting from commercially available compounds, are discussed.Treatment of diethyl 2-chloromalonate with thiolate anions followed by LiAlH4 reduction gave 9a,b,c in nearly 30percent overall
Synthesis of Unsymmetrical Functionalised Organic Sulphides
Singh, Harjit,Batra, Manohar S.,Singh, Paramjit
, p. 131 - 136 (2007/10/02)
Acyclic thioiminium salts and the condensed thiazolium salts in the presence of aqueous sodium hydroxide as such or under base catalyzed phase transfer catalysis conditions react with appropiate organic halides to provide corresponding unsymmetrical functionalized organic sulphides.With aqueous sodium hydroxide, thioiminium salts provide the disulphides corresponding to incipient thiol.
Synthesis of Unsymmetrical Thioethers Using Solid-Liquid Phase-transfer Catalysis
Singh, Paramjit,Batra, Manohar S.,Singh, Harjit
, p. 484 (2007/10/02)
The title compounds have been synthesised from appropriate organic halides and thioimminium salts (1) in moderate to good yields under solid-liquid phase-transfer catalysis using Triethylbenzylammonium chloride (TEBA) as a catalyst, solid KOH as a base in chloroform.
