176098-17-2Relevant articles and documents
Stereoselective intermolecular [2+2] photocycloaddition reactions of tetrahydrophthalic anhydride and derivatives with alkenols and alkynols
Booker-Milburn, Kevin I.,Cowell, Justin K.,Delgado Jimenez,Sharpe, Andrew,White, Andrew J.
, p. 5875 - 5888 (1999)
Intermolecular [2+2] photocycloaddition of a variety of alken- and alkyn-3-ols with 3,4,5,6-tetrahydrophthalic anhydride (THPA) and the related imide (THPI) gave the corresponding cyclobutanes and cyclobutenes in high yield. Irradiation times were relatively short and stereoselectivities as high as 10/1 for the cyclobutane examples.
A Small-Footprint, High-Capacity Flow Reactor for UV Photochemical Synthesis on the Kilogram Scale
Elliott, Luke D.,Berry, Malcolm,Harji, Bashir,Klauber, David,Leonard, John,Booker-Milburn, Kevin I.
, p. 1806 - 1811 (2016)
The development of a highly compact and powerful reactor for synthetic organic photochemistry is described enabling a 10-fold reduction in reaction times, with up to 30% more power efficiency than previous fluorinated ethylene propylene tube reactors. Two