Chemical Communications p. 249 - 251 (1996)
Update date:2022-08-11
Topics:
Booker-Milburn, Kevin I.
Cowell, Justin K.
Sharpe, Andrew
Delgado Jimenez
Intermolecular photochemical [2 + 2] cycloaddition of a variety of alken- and alkyn-3-ols with 3,4,5,6-tetrahydrophthalic anhydride (THPA) and the related imide 4 gave the corresponding cyclobutanes and cyclobutenes in high yield, after relatively short irradiation times, with stereoselectivities as high as 10:1 for the cyclobutane examples.
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