Tetrahydrophthalic anhydride and imide: Remarkably efficient partners in photochemical [2 + 2] cycloaddition reactions with alkenols and alkynols

DOI: 10.1039/CC9960000249

Source and publish data:

Chemical Communications p. 249 - 251 (1996)

Update date:2022-08-11

Topics:

Authors:

Booker-Milburn, Kevin I.

Cowell, Justin K.

Sharpe, Andrew

Delgado Jimenez

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Article abstract of DOI:10.1039/CC9960000249

Intermolecular photochemical [2 + 2] cycloaddition of a variety of alken- and alkyn-3-ols with 3,4,5,6-tetrahydrophthalic anhydride (THPA) and the related imide 4 gave the corresponding cyclobutanes and cyclobutenes in high yield, after relatively short irradiation times, with stereoselectivities as high as 10:1 for the cyclobutane examples.

Full text of DOI:10.1039/CC9960000249

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