18002-79-4Relevant academic research and scientific papers
First synthesis of the three isomeric parent disilacyclohexanes. An improved preparation of methylene di-grignard
Gudnason, Palmar I.,Arnason, Ingvar
supporting information; experimental part, p. 2015 - 2017 (2009/09/25)
Ring closure of 1,5-dibromo-1,5-disilapentane with methylene di-Grignard was the key step in the preparation of the parent 1,3-disilacyclohexane. For that purpose, the preparation of methylene di-Grignard has been improved and simplified. The successful s
