18621-76-6Relevant academic research and scientific papers
No-D NMR (No-Deuterium Proton NMR) spectroscopy: A simple yet powerful method for analyzing reaction and reagent solutions
Hoye, Thomas R.,Eklov, Brian M.,Ryba, Troy D.,Voloshin, Mikhail,Yao, Letitia J.
, p. 953 - 956 (2007/10/03)
(Equation presented) The title technique is a convenient and powerful method for directly monitoring or assaying any reaction mixture or reagent solution. Examples of some common processes (Fischer esterification, lithiation, butyllithium/THF compatibility, olefin metathesis, and a quantification assay), each interrogated in its native solvent, are presented. The spectral data are easy to acquire, and the information content makes a compelling case for routine use of No-D NMR spectroscopy.
