186519-15-3Relevant academic research and scientific papers
Formation of vinyl and dithioformate metallacycles by insertion of an ester-functionalized alkyne or carbon disulfide into an Fe-H bond: Crystal structure of cis-[Fe(CH=CHCOOMe)(Ph2PCH2CH2PPh2)2][BF4]
Almeida, Silvia S. P.,Duarte, Maria T.,Ribeiro, Luisa M. D.,Gormley, Fiona,Galvao, Adeline M.,Frausto Da Silva, Joao J. R.,Pombeiro, Armando J. L.
, p. 63 - 66 (1996)
Treatment of a THF solution of trans-[FeHCl(dppe)2] (dppe = Ph2PCH2CH2PPh2) with HC≡CCOOMe or CS2, in the presence of T1[BF4], forms the vinyl complex cis-[Fe(CH=CHCOOMe)(dppe)2][BF4] or the η2-dithioformate compound cis-[Fe(η2-S2CH)(dppe)2][BF4] respectively. The molecular structure of the former is authenticated by X-ray diffraction analysis.
