210241-76-2Relevant academic research and scientific papers
Microwave enhanced solution synthesis of 1,4-benzodiazepin-5-ones
Santagada, Vincenzo,Perissutti, Elisa,Fiorino, Ferdinando,Vivenzio, Beniamino,Caliendo, Giuseppe
, p. 2397 - 2400 (2001)
Some 2-methyl-1,4-benzodiazepin-5-ones have been synthesized by the application of microwave irradiation. Conventional heating and microwave irradiation of the reactions were compared. Synthesis by microwave irradiation gave the desired compounds in better yields than those obtained by conventional heating. The overall times for the syntheses were considerably reduced.
A Facile Synthesis of 2-Methyl-1,4-benzodiazepin-5-ones via Intramolecular Azide Cycloaddition
Broggini, Gianluigi,Zecchi, Gaetano,Molteni, Giorgio
, p. 809 - 810 (2007/10/03)
New 2-methyl-1,4-benzodiazepin-5-ones have been synthesized through a short and efficient procedure, which involves an intramolecular azide cycloaddition as the key step.
