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222713-05-5

1H-Isoindol-1-one, 2,3-dihydro-2-(phenylmethyl)-3-(phenylthio)- is a chemical with a specific purpose. Lookchem provides you with multiple data and supplier information of this chemical.

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  • 222713-05-5 Structure

  • Basic information

    1. Product Name: 1H-Isoindol-1-one, 2,3-dihydro-2-(phenylmethyl)-3-(phenylthio)-
    2. Synonyms:
    3. CAS NO:222713-05-5
    4. Molecular Formula: C21H17NOS
    5. Molecular Weight: 331.438
    6. EINECS: N/A
    7. Product Categories: N/A
    8. Mol File: 222713-05-5.mol

  • Chemical Properties

    1. Melting Point: N/A
    2. Boiling Point: N/A
    3. Flash Point: N/A
    4. Appearance: N/A
    5. Density: N/A
    6. Refractive Index: N/A
    7. Storage Temp.: N/A
    8. Solubility: N/A
    9. CAS DataBase Reference: 1H-Isoindol-1-one, 2,3-dihydro-2-(phenylmethyl)-3-(phenylthio)-(CAS DataBase Reference)
    10. NIST Chemistry Reference: 1H-Isoindol-1-one, 2,3-dihydro-2-(phenylmethyl)-3-(phenylthio)-(222713-05-5)
    11. EPA Substance Registry System: 1H-Isoindol-1-one, 2,3-dihydro-2-(phenylmethyl)-3-(phenylthio)-(222713-05-5)

  • Safety Data

    1. Hazard Codes: N/A
    2. Statements: N/A
    3. Safety Statements: N/A
    4. WGK Germany:
    5. RTECS:
    6. HazardClass: N/A
    7. PackingGroup: N/A
    8. Hazardous Substances Data: 222713-05-5(Hazardous Substances Data)

222713-05-5 Usage

Check Digit Verification of cas no

The CAS Registry Mumber 222713-05-5 includes 9 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 6 digits, 2,2,2,7,1 and 3 respectively; the second part has 2 digits, 0 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 222713-05:
(8*2)+(7*2)+(6*2)+(5*7)+(4*1)+(3*3)+(2*0)+(1*5)=95
95 % 10 = 5
So 222713-05-5 is a valid CAS Registry Number.

222713-05-5Relevant articles and documents

A new entry for the preparation of substituted aromatic carbonyl compounds mediated by Samarium(II) iodide

Yoda, Hidemi,Kohata, Naoki,Takabe, Kunihiko

, p. 1087 - 1094 (2003)

A new route to substituted aromatic lactones and lactams via SMI2-promoted desulfurization is described. Direct replacement of the phenylthio substituent by hydroxyalkylated groups featuring the novel accessible process for the construction of continuous quaternary carbon centers could be accomplished when the same type of reactions was undertaken with carbonyl compounds in the presence of SmI2.

Bifurcated synthesis of methylene-lactone- And methylene-lactam-fused spirolactams via electrophilic amide allylation of γ-phenylthio-functionalized γ-lactams

Iijima, Ayumi,Inuzuka, Toshiyasu,Makino, Koki,Sengoku, Tetsuya,Yoda, Hidemi

supporting information, p. 2769 - 2775 (2020/12/11)

New synthetic methods for spirolactams bearing an α-methylene-γ-butyrolactone or its analogous methylene-lactam have been developed. The allylation of γ-phenylthio-functionalized γ-lactams with 2-(acetoxy)methyl acrylamides was accomplished by using 2.5 equivalents of NaH to give the corresponding adducts in excellent yields. The remaining phenylthio group was substituted with a hydroxy group by treatment with CuBr, and the resulting γ-hydroxyamides were cyclized under acidic conditions to afford the corresponding methylene-lactam-fused spirolactams in high yields. On the other hand, methylene-lactone-fused spirolactams could be delivered from the allyl adducts in high yields through a sequential N-Boc protection/desulfinative lactonization.

SmI2-promoted tandem desulfurization and reductive coupling reactions of aromatic lactams with carbonyl compounds

Yoda, Hidemi,Ujihara, Yasuaki,Takabe, Kunihiko

, p. 9225 - 9228 (2007/10/03)

Treatment of sulfur-substituted aromatic lactams with carbonyl compounds in the presence of samarium(II) diiodide was found to undergo novel tandem desulfurization and reductive coupling reactions to generate α-hydroxyalkylated lactams in high yield. Ster

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