247153-85-1Relevant articles and documents
Azo-containing tertiary phosphines: synthesis, reactivity and structural characterisation
Alder, Mark J.,Cross, Wendy I,Flower, Kevin R.,Pritchard, Robin G.
, p. 2563 - 2574 (2007/10/03)
6-Bromo-2-methoxynaphthalene 1 was converted into 6-diphenylphosphanyl-2-methoxynaphthalene 2a by preparing its Grignard and quenching with PPh2Cl. Compound 2a was demethylated on refluxing in HBr yielding 6-(diphenylphosphanyl)naphthalen-2-ol 2b in good