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24817-51-4

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24817-51-4 Usage

InChI:InChI=1/C13H18O2/c1-3-11(2)13(14)15-10-9-12-7-5-4-6-8-12/h4-8,11H,3,9-10H2,1-2H3

24817-51-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-phenylethyl 2-methylbutanoate

1.2 Other means of identification

Product number -
Other names 2-phenylethyl 2-methylbutyrate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Food additives -> Flavoring Agents
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:24817-51-4 SDS

24817-51-4Synthetic route

2-oxo-3(RS)-methylvaleric acid
1460-34-0

2-oxo-3(RS)-methylvaleric acid

2-phenylethanol
60-12-8

2-phenylethanol

2-methyl-butanoic acid 2-phenylethyl ester
24817-51-4

2-methyl-butanoic acid 2-phenylethyl ester

Conditions
ConditionsYield
With 3-nitro(diacetoxyiodo)benzene In dichloromethane at 20℃; for 24h; Sealed tube; Darkness; chemoselective reaction;85%
1-butylene
106-98-9

1-butylene

carbon monoxide
201230-82-2

carbon monoxide

2-phenylethanol
60-12-8

2-phenylethanol

A

2-methyl-butanoic acid 2-phenylethyl ester
24817-51-4

2-methyl-butanoic acid 2-phenylethyl ester

B

phenethylpentanoate
7460-74-4

phenethylpentanoate

Conditions
ConditionsYield
With toluene-4-sulfonic acid; palladium(II) bromide; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In toluene at 100℃; under 30003 Torr; for 20h; Overall yield = 96 %; regioselective reaction;
butene-2
107-01-7

butene-2

carbon monoxide
201230-82-2

carbon monoxide

2-phenylethanol
60-12-8

2-phenylethanol

A

2-methyl-butanoic acid 2-phenylethyl ester
24817-51-4

2-methyl-butanoic acid 2-phenylethyl ester

B

phenethylpentanoate
7460-74-4

phenethylpentanoate

Conditions
ConditionsYield
With toluene-4-sulfonic acid; palladium(II) bromide; 2-(dicyclohexylphosphino)-1-(2-methoxyphenyl)-1H-pyrrole In toluene at 100℃; under 30003 Torr; for 20h; Overall yield = 90 %; regioselective reaction;

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