25180-82-9Relevant academic research and scientific papers
A highly efficient one-pot method for the synthesis of thioureas and 2-imino-4-thiazolidinones under microwave conditions
Chau, Chi-Min,Chuan, Tzu-Jung,Liu, Kuan-Miao
, p. 1276 - 1282 (2014/01/06)
A one-pot synthesis of symmetrical and unsymmetrical substituted thioureas and 2-imino-4-thiazolidinones from simple starting materials under microwave irradiation and solventless conditions without base additives is presented. Various di- and trisubstituted thioureas are obtained in good yields in a few minutes. The sequential, three-component, one-pot synthesis of 2-imino-4-thiazolidinone derivatives is also studied, with satisfactory results obtained.
A novel atom-efficient, one-pot synthesis of sulfonylguanidines and sulfamoylguanidines
Lange, Jos H.M.,Verhoog, Stefan,Sanders, Hans J.,Van Loevezijn, Arnold,Kruse, Chris G.
experimental part, p. 3198 - 3200 (2011/06/28)
An expedient one-pot procedure for the atom-efficient production of a variety of sulfonylguanidines and sulfamoylguanidines under mild conditions is described. The route constitutes an important alternative to current methods.
Self-indicating amine scavenger resins
Cho, Jin Ku,White, Peter D.,Klute, Wolfgang,Dean, Tony W.,Bradley, Mark
, p. 502 - 503 (2007/10/03)
Self-indicating methylisocyanate resin, which functions as both a scavenger and an indicator for amines, was used for in-situ reaction monitoring and purification of a urea based library.
1-(Methyldithiocarbonyl)imidazole: A useful thiocarbonyl transfer reagent for synthesis of substituted thioureas
Mohanta, Pramod K.,Dhar, Sanchita,Samal,Ila,Junjappa
, p. 629 - 637 (2007/10/03)
1-(Methyldithiocarbonyl)imidazole 1 and its N-methyl quaternary salt 2 have been shown to be efficient methyldithiocarbonyl and thiocarbonyl transfer reagents for the synthesis of dithiocarbamates, symmetrical and unsymmetrical mono-, di- and tri-substituted thioureas in high yields under mild and simple non-hazardous reaction conditions. (C) 2000 Elsevier Science Ltd.
