260261-48-1Relevant academic research and scientific papers
Synthesis of labelled 1-azafagomine
Hansen, Steen Uldall,Bols, Mikael
, p. 3323 - 3325 (2007/10/03)
(3,4-trans-4,5-trans)-4,5-Dihydroxy-3-(hydroxymethyl)hexahydro-(3- 13C)pyridazine (azafagomine, 1a) was synthesised in 7 steps starting from (2-13C) malonic acid 5a through conversion to pentadienoic acid and Diels-Alder reaction with 4-phenyl-1,2,4-triazole-3,5-dione, reduction, epoxidation, epoxide hydrolysis and deprotection. The Royal Society of Chemistry 1999.
