288623-03-0

Basic information

• Product Name: 2H-1,3-Oxazine-2,6(3H)-dione,dihydro-4-(1-methylethyl)-,(4R)-(9CI)
• Synonyms: 2H-1,3-Oxazine-2,6(3H)-dione,dihydro-4-(1-methylethyl)-,(4R)-(9CI)
• CAS NO: 288623-03-0
• Molecular Formula: C7H11NO3
• Molecular Weight: 0
• Product Categories: ISOPROPYL
• Mol File: 288623-03-0.mol

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 2H-1,3-Oxazine-2,6(3H)-dione,dihydro-4-(1-methylethyl)-,(4R)-(9CI)(CAS DataBase Reference)
• NIST Chemistry Reference: 2H-1,3-Oxazine-2,6(3H)-dione,dihydro-4-(1-methylethyl)-,(4R)-(9CI)(288623-03-0)
• EPA Substance Registry System: 2H-1,3-Oxazine-2,6(3H)-dione,dihydro-4-(1-methylethyl)-,(4R)-(9CI)(288623-03-0)

Safety Data

• Hazardous Substances Data: 288623-03-0(Hazardous Substances Data)

Upstream product

• 90105-46-7 benzyl (S)-(1-diazo-4-methyl-2-oxopentan-3-yl)carbamate 
• 67865-71-8 (S)-3-(tert-butoxycarbonylamino)-1-diazo-4-methylpentan-2-one 
• 13734-41-3 t-Boc-L-valine 
• 179412-79-4 (S)-3-((tert-butoxycarbonyl)amino)-4-methylpentanoic acid 
• 245323-45-9 (3S)-N-(benzyloxycarbonyl)-3-amino-4-methylpentanoic acid 
• 32315-10-9 bis(trichloromethyl) carbonate 
• 109446-56-2 3-benzyloxycarbonylamino-4-methyl-valeric acid 
• 1149-26-4 (S)-N-(benzyloxycarbonyl)valine 

Relevant articles and documents

Single-Step, Rapid, and Mild Synthesis of β-Amino Acid N-Carboxy Anhydrides Using Micro-Flow Technology

β-Amino acid N-carboxy anhydrides (β-NCAs) are rarely used in the synthesis of β-peptides, which is due mainly to the poor availability of these potentially useful substrates. Herein, we describe the heretofore challenging synthesis of β-NCAs via a single

METHOD OF SYNTHESIZING N-CARBOXYANHYDRIDE USING FLOW REACTOR

PROBLEM TO BE SOLVED: To provide a synthesis method that allows high-yield continuous production of a compound of interest in synthesis and production of N-carboxyanhydride (NCA) and the like using a flow reactor. SOLUTION: In a synthesis method using a flow reactor 100, a basic solution adjusted in advance to a pH of 7-14 becomes acidic with a pH of 0-7, or an acidic solution adjusted in advance to a pH of 0-7 becomes basic with a pH of 7-14, within 60 seconds after the start of mixture of at least two ingredient solutions. SELECTED DRAWING: Figure 1 COPYRIGHT: (C)2020,JPOandINPIT

Micro-flow synthesis of β-amino acid derivatives: Via a rapid dual activation approach

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