3101-50-6Relevant articles and documents
METHYLENATION OF CARBONYL COMPOUNDS WITH METHYLENEDIMAGNESIUM IODIDE IN THE PRESENCE OF Et2AlCl
Dzhemilev, U. M.,Ibragimov, A. G.,Morozov, A. B.,Muslukhov, R. R.,Tolstikov, G. A.
, p. 2350 - 2352 (2007/10/02)
A method has been developed for the methylenation of carbonyl compounds with methylenedimagnesium iodide in the presence of Et2AlCl in 35-70percent yield.In the presence of catalytic amounts of Ti and Pd complexes the yield of methylenation products is increased by 15-20percent.