339293-46-8Relevant academic research and scientific papers
Synthesis and characterization of 5-amino-1,3,6-trinitro-1H-benzo[d]imidazol-2(3H)-one as an energetic material
Ma, Congming,Liu, Zuliang,Yao, Qizheng
, p. 42215 - 42219 (2015/02/05)
Two synthetic routes for the preparation of 5-amino-1,3,6-trinitro-1H-benzo[d]imidazol-2(3H)-one (2) as an energetic material have been revealed. Direct nitration of 5-amino-1H-benzo[d]imidazol-2(3H)-one (1) gave the trinitrated compound 2 in a poor yield of 11%; and similarly using 1 as starting material, 2 was obtained by N-protected reaction, nitration, deprotection and again nitration reaction with an overall-yield of 48%. All structures of 2 and relevant compounds were determined by IR, 1H NMR, 13C NMR spectroscopy, MS and elemental analysis. Theoretical calculations showed that the detonation properties of compound 2 (D = 7.78 km s-1, P = 27.05 GPa) were satisfactory, compared with 2,4,6-trinitrotoluene (TNT, D = 7.21 km s-1, P = 22.49 GPa). This journal is
MORPHOLINONE COMPOUNDS AS FACTOR IXA INHIBITORS
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Page/Page column 199, (2010/06/20)
The present invention provides a compound of Formula (I) as described herein, or a pharmaceutically acceptable salt or a solvate thereof. The present invention also provides pharmaceutical compositions comprising one or more said compounds, and methods fo
