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34810-13-4

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34810-13-4 Usage

Uses

9-Anthraldehyde oxime was used in preparation of new triosmium cluster [Os3(CO)11(C14H9CN)].

General Description

Gallium triflate catalyzed dehydration of 9-anthraldehyde oxime to nitrile is reported.

Check Digit Verification of cas no

The CAS Registry Mumber 34810-13-4 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 3,4,8,1 and 0 respectively; the second part has 2 digits, 1 and 3 respectively.
Calculate Digit Verification of CAS Registry Number 34810-13:
(7*3)+(6*4)+(5*8)+(4*1)+(3*0)+(2*1)+(1*3)=94
94 % 10 = 4
So 34810-13-4 is a valid CAS Registry Number.
InChI:InChI=1/C15H11NO/c17-16-10-15-13-7-3-1-5-11(13)9-12-6-2-4-8-14(12)15/h1-10,17H/b16-10+

34810-13-4 Well-known Company Product Price

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  • Aldrich

  • (301612)  9-Anthraldehydeoxime,predominantlysyn  99%

  • 34810-13-4

  • 301612-10G

  • 1,124.37CNY

  • Detail

34810-13-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 19, 2017

Revision Date: Aug 19, 2017

1.Identification

1.1 GHS Product identifier

Product name 9-Anthraldehyde oxime

1.2 Other means of identification

Product number -
Other names 9-Anthraldehyde oxim

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:34810-13-4 SDS

34810-13-4Relevant articles and documents

Aerobic oxidation of primary amines to amides catalyzed by an annulated mesoionic carbene (MIC) stabilized Ru complex

Yadav, Suman,Reshi, Noor U Din,Pal, Saikat,Bera, Jitendra K.

, p. 7018 - 7028 (2021/11/17)

Catalytic aerobic oxidation of primary amines to the amides, using the precatalyst [Ru(COD)(L1)Br2] (1) bearing an annulated π-conjugated imidazo[1,2-a][1,8]naphthyridine-based mesoionic carbene ligand L1, is disclosed. This catalytic protocol is distinguished by its high activity and selectivity, wide substrate scope and modest reaction conditions. A variety of primary amines, RCH2NH2 (R = aliphatic, aromatic and heteroaromatic), are converted to the corresponding amides using ambient air as an oxidant in the presence of a sub-stoichiometric amount of KOtBu in tBuOH. A set of control experiments, Hammett relationships, kinetic studies and DFT calculations are undertaken to divulge mechanistic details of the amine oxidation using 1. The catalytic reaction involves abstraction of two amine protons and two benzylic hydrogen atoms of the metal-bound primary amine by the oxo and hydroxo ligands, respectively. A β-hydride transfer step for the benzylic C-H bond cleavage is not supported by Hammett studies. The nitrile generated by the catalytic oxidation undergoes hydration to afford the amide as the final product. This journal is

Corresponding amine nitrile and method of manufacturing thereof

-

Paragraph 0135; 0136; 0137; 0143, (2018/05/07)

The invention relates to a manufacturing method of nitrile. Compared with the prior art, the manufacturing method has the characteristics of significantly reduced using amount of an ammonia source, low environmental pressure, low energy consumption, low production cost, high purity and yield of a nitrile product and the like, and nitrile with a more complex structure can be obtained. The invention also relates to a method for manufacturing corresponding amine from nitrile.

Palladium-catalyzed synthesis of primary benzamides from aryl bromides via a cyanation and hydration sequence

Sharif, Muhammad,Wu, Xiao-Feng

, p. 21001 - 21004 (2015/03/30)

An interesting and effective procedure for the synthesis of benzamides from aryl bromides has been developed. In the presence of a palladium catalyst, various primary benzamides have been produced in moderate to excellent yields in a one-pot one-step manner.

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