3676-98-0Relevant articles and documents
Convenient synthesis of dicyclohexyldithiophosphinic acid
Jia, Cai,Yu, Fengxian,Wang, Fang,Wu, Wangsuo,Chen, Jing
experimental part, p. 2036 - 2041 (2010/08/13)
Dicyclohexyldithiophosphinic acid was synthesized by a three-step strategy through the Grignard reaction of PSCl3 with cyclo-C6H 11MgBr and the P-P bond-cleavage reaction of the intermediate. The 1H NMR data of ammonium dicyclohexyldithiophosphinate 4 and dicyclohexyldithiophosphinic acid 5 were characterized by 1H- 1H correlation spectra. Copyright Taylor & Francis Group, LLC.