36957-54-7Relevant articles and documents
A MILD AND FACILE SYNTHESIS OF ALKYL- AND ARYLPHOSPHONYL DICHLORIDES UNDER NEUTRAL CONDITIONS. REACTION OF BIS(TRIMETHYLSILYL) PHOSPHONATES WITH PCl5
Morita, Tsuyoshi,Okamoto, Yoshiki,Sakurai, Hiroshi
, p. 435 - 438 (1980)
Bis(trimethylsilyl) phosphonates, which are prepared from the dialkyl esters with chlorotrimethylsilane/sodium iodide, are transformed in high yields into the corresponding phosphonyl dichlorides on the treatment with phosphorus pentachloride under mild and neutral conditions.