36998-40-0Relevant articles and documents
Trimethylsilyloxide-Catalysed Peterson Olefinations with 2,2-Bis(trimethylsilyl)-1,3-dithiane
Manvar, Atul,O'Shea, Donal F.
supporting information, p. 7259 - 7263 (2015/11/25)
The synthesis of the reagent 2,2-bis(trimethylsilyl)-1,3-dithiane was directly achieved in an excellent yield from 1,3-dithiane in one step. The bench-stable reagent can be utilized for Peterson olefinations using either TMSOK/Bu4NCl or fluorid
Counterattack Reagent: Hexamethyldisilane in a Direct Synthesis of Ketene Dithioacetals and 2-Trimethylsilyl-1,3-dithiane Derivatives from 1,3-Dithiane
Hwu, Jih Ru,Lee, Taekyo,Gilbert, Bryant A.
, p. 3219 - 3224 (2007/10/02)
A novel method has been developed for the direct synthesis of ketene dithioacetals and 2-trimethylsilyl-1,3-dithiane derivatives from 1,3-dithiane.Treatment of 1,3-dithiane (1.0 mol equiv.) with BuLi (1.1 mol equiv.), HMPA (4.0 mol equiv.), and Me3SiSiMe3
A Modified Synthesis of Alkylidene-1,3-dithianes
Chamchaang, W.,Prankprakma, V.,Tarnchompoo, B.,Thebtaranonth, C.,Thebtaranonth, Y.
, p. 579 - 580 (2007/10/02)
-