38926-45-3Relevant articles and documents
2. 3, 5, 6 - Tetraaminopyridine preparation method
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Paragraph 0012; 0025-0033, (2019/06/05)
The invention discloses a method for 2, 3, 5, 6 - four-aminopyridine preparation method. The invention relates to 2, 6 - diamino - 3, 5 - dinitro-pyridine as raw materials, in order to water-free formic acid binds reducing agent, in the presence of Pd/C catalyst reduction reaction, thus under normal pressure to obtain 2, 3, 5, 6 - four-aminopyridine. For the preparation process of the invention 2, 3, 5, 6 — four-aminopyridine, purity of 99% or more, the yield is 85 - 95%. The invention compared with the prior art, the reaction carried out at normal pressure, to avoid the high pressure catalytic hydrogenation reduction of the safety factor, the mild conditions in the reaction process, safe and convenient operation, and high product purity, it is suitable for industrial production.
PROCESSES FOR PREPARING MONOMER COMPLEXES
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Page/Page column 22-23, (2010/11/24)
Disclosed are processes for preparing monomer complexes that include contacting 2,3,5,6-tetraaminopyridine free base in water with 2,5-dihydroxy terephthalic acid dipotassium salt to form an aqueous mixture, and adjusting the pH of the aqueous mixture to