43016-41-7Relevant academic research and scientific papers
Superbasic system CsOH/DMSO as a reagent for a fast one-step synthesis of symmetrical dialkyl trithiocarbonates
Yousefi, Ali
, p. 672 - 677 (2015)
Symmetrical dialkyl trithiocarbonates were readily synthesized in excellent yields by one-step reaction of carbon disulfide and various alkyl halides under mild reaction conditions in the presence of cesium hydroxide as a super basic system. This method provides a synthesis of symmetrical dialkyl trithiocarbonates in short reaction times without the use of highly toxic starting materials.
An Efficient and Straightforward Access to Symmetrical Dialkyl Trithiocarbonates Using a Basic Task-Specific Ionic Liquid and Carbon Disulfide
Sayyahi, Soheil,Moonesi, Saeid,Fallah-Mehrjardi, Mehdi
, p. 1718 - 1722 (2015/11/02)
We report an efficient one-pot route for the synthesis of symmetrical dialkyl trithiocarbonates from alkyl halides using carbon disulfide and a basic ionic liquid 1,1′-bis-methyl-3, 3-methylene-bisimidazolium dihydroxide as a reagent and phase-transfer catalyst.
K3PO4-mediated one-pot synthesis of symmetrical trithiocarbonates
Movassagh, Barahman,Alapour, Saba
, p. 222 - 226 (2013/08/26)
A new procedure has been developed for synthesis of symmetrical trithiocarbonates by one-pot reaction of carbon disulfide, and various alkyl halides in dimethylformamide using K3PO4 as an inexpensive and effective reagent.
A novel one-step synthesis of symmetrical dialkyl trithiocarbonates in the presence of phase-transfer catalysis
Kiasat, Ali Reza,Mehrjardi, Mehdi Fallah
experimental part, p. 639 - 642 (2009/05/11)
Symmetrical trithiocarbonates were directly obtained, in moderate to excellent isolated yields, by the reaction of various primary, secondary, allylic and benzylic halides or alkyl tosylates with a suspension of granulated KOH and alumina in CS2 under phase-transfer catalysis. In this manner, cyclic trithiocarbonates such as 1,3-dithiolane-2-thione can also be prepared without formation of any polymeric by-products.
A search for radioprotective agents. XXVII. Synthesis of some trithiocarbonates
Tulecki,Golus
, p. 259 - 261 (2007/10/05)
The following novel trithiocarbonates were obtained in the reaction of exchange of potassium trithiocarbonate and appropriate halogenated compounds: di(4 bromobenzyl), di(4 cyanobenzyl), di(1 carbethoxybenzimidazolyl 2 methyl, and di(1 carbmethoxybenzimidazolyl 2 methyl) trithiocarbonates. The compounds will be tested for their radioprotective properties.
