5180-31-4Relevant academic research and scientific papers
Direct and facile synthesis of acyl azides from carboxylic acids using the trichloroisocyanuric acid-triphenylphosphine system
Akhlaghinia, Batool,Rouhi-Saadabad, Hamed
, p. 181 - 185 (2013/05/09)
A mild, efficient, and practical method for the one-step synthesis of acyl azides from carboxylic acids using a safe and inexpensive mixed reagent, trichloroisocyanuric acid-triphenylphosphine, is described.
Direct synthesis of acyl azides from carboxylic acids using 2-azido-l,3-dimethylimidazolinium chloride
Kitamura, Mitsuru,Tashiro, Norifumi,Takamoto, Yusuke,Okauchi, Tatsuo
scheme or table, p. 731 - 733 (2011/01/08)
Acyl azides were directly synthesized from carboxylic acids by the treatment with 2-azido-l,3-dimethylimidazolinium chloride (ADMC, 1) and amine. This procedure resulted in acyl azides in good yields and was applied to the amidation of amino acid derivatives without racemization of the products.
A new facile and rapid synthesis of acyl azides under solvent-free conditions
Mallakpour,Hajipour,Vahabi
, p. 1234 - 1235 (2007/10/03)
A rapid and simple method for the preparation of acyl azides is described. The reaction is carried out under solvent-free conditions from the reaction of acid chlorides with sodium azide supported on silica gel.
One-flask conversion of carboxylic acids into carbamoyl azides
Froyen
, p. 4549 - 4561 (2007/10/03)
Carbamoyl azides can be generated in high yields from the corresponding carboxylic acid and triphenylphosphine by adding NCS, followed by sodium azide and triethylamine hydrochloride.
