185691-72-9Relevant academic research and scientific papers
Controlled conversion of phenylacetic acids to phenylacetonitriles or benzonitriles using bis(2-methoxyethyl)aminosulfur trifluoride
Kangani, Cyrous O.,Day, Billy W.,Kelley, David E.
, p. 914 - 918 (2008/09/17)
A mild, efficient, and practical method for the one-step synthesis of benzonitriles from phenylacetic acids using bis(2-methoxyethyl)aminosulfur trifluoride is described. The reaction was easily extended to the synthesis of the corresponding phenylacetonitriles by inclusion of triethylphosphine.
One-flask conversion of carboxylic acids into carbamoyl azides
Froyen
, p. 4549 - 4561 (2007/10/03)
Carbamoyl azides can be generated in high yields from the corresponding carboxylic acid and triphenylphosphine by adding NCS, followed by sodium azide and triethylamine hydrochloride.
