52447-23-1Relevant articles and documents
Precise synthesis of novel chain-end-functionalized polystyrenes with a definite number of perfluorooctyl groups and their surface characterization
El-Shehawy, Ashraf A.,Yokoyama, Hideaki,Sugiyama, Kenji,Hirao, Akira
, p. 8285 - 8299 (2005)
We have successfully synthesized two types of chain-end-functionalized polystyrenes with a definite number of C8F17 groups that are dendritically distributed and linearly aligned in a double line. They are referred to as D and L type
Preparation method of fluorine-containing carboxylic acid
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Paragraph 0046; 0048-0049, (2020/07/12)
The invention discloses a preparation method of fluorine-containing carboxylic acid. The method comprises the following steps: reacting fluorine-containing carboxylate used as a raw material with an acylating chlorination reagent to obtain a corresponding mixture of fluorine-containing acyl chloride and fluorine-containing anhydride, and hydrolyzing and drying the mixture of fluorine-containing acyl chloride and fluorine-containing anhydride to obtain high-purity fluorine-containing carboxylic acid. The method provided by the invention is suitable for post-treatment of fluorine-containing carboxylic acid prepared by a fluorine-containing olefin (monoolefine, diene, cycloolefin and the like) oxidation method, replaces the traditional strong acid acidification and ether continuous extractionprocess, and is simpler, more convenient and more applicable; and the method can also be used for recovering and purifying a fluorine-containing carboxylate emulsifier. The purity of the fluorine-containing carboxylic acid prepared by the method can reach 98% or above.
SYNTHESES OF PERFLUOROALKYL N-POLYETHOXYLATED AMIDES
Afzal, Jalees,Fung, B. M.,O'Rear, Edgar A.
, p. 385 - 394 (2007/10/02)
Monodisperse perfluoroalkyl N-polyethoxylated amides, CnF2n+1CONH(CH2CH2O)mH, with n = 6, 7, 8 and 9 and m = 2, 3, and 4 are potential nonionic fluorinated surfactants.The syntheses of these comounds are described.