5358-27-0Relevant academic research and scientific papers
Stereoselective synthesis of all-trans-, (13Z)- and (9-nor)-retinoic acids via Stille reaction
Thibonnet, Jér?me,Abarbri, Mohamed,Duchêne, Alain,Parrain, Jean-Luc
, p. 141 - 143 (2007/10/03)
Stereoselective construction of retinoic acid and certain analogues were achieved through two successive Stille reactions. First, the coupling of (E)- 1,2-bis(tributylstannyl)ethene and (Z)- or (E)-tributylstannyl 3-iodoalk-2- enoates was performed followed by iododestannylation. The second step involved another vinyltin which was synthesised by stannylmetallation of the Negishi dienyne derived from β-ionone.
