53687-75-5

Basic information

• Product Name: phenyl-2, dihydro-3,4 benzo (b) 5H-azepine
• Synonyms: phenyl-2, dihydro-3,4 benzo (b) 5H-azepine
• CAS NO: 53687-75-5
• Molecular Weight: 221.302
• Mol File: 53687-75-5.mol
• Article Data: 3

Chemical Properties

• CAS DataBase Reference: phenyl-2, dihydro-3,4 benzo (b) 5H-azepine(CAS DataBase Reference)
• NIST Chemistry Reference: phenyl-2, dihydro-3,4 benzo (b) 5H-azepine(53687-75-5)
• EPA Substance Registry System: phenyl-2, dihydro-3,4 benzo (b) 5H-azepine(53687-75-5)

Safety Data

• Hazardous Substances Data: 53687-75-5(Hazardous Substances Data)

Upstream product

• 7469-40-1 1-phenyl-3,4-dihydronaphthalene 
• 935-64-8 1-phenyl-1-cyclobutanol 
• 615-36-1 2-bromoaniline 
• 615-43-0 2-iodophenylamine 
• 40164-53-2 1,4-diphenyl-1-butyne 

Downstream Products

• 71718-77-9 phenyl-2, tetrahydro-2,3,4,5 benzo (b) 1H-azepine 

Relevant articles and documents

Synthesis method of 2-aryl benzazepine and derivatives thereof

The invention relates to a synthesis method of 2-aryl benzazepine and derivatives thereof, the method comprises the following steps: stirring and reacting 2-halogenated aniline and aryl cyclobutanol as reaction substrates, palladium chloride as a catalyst, tricyclohexylphosphine as a ligand, cesium carbonate as alkali and ultra-dry toluene as a solvent in a nitrogen atmosphere at 110 DEG C for 12 hours. The method has the advantages of simple and easily available raw materials, relatively mild reaction conditions, wide substrate universality, novel preparation process, low energy consumption and the like.

New method for synthesis of 2-substituted 2,3,4,5-tetrahydrobenzo(b)-1H-azepines

-