65002-17-7Relevant articles and documents
Thiol compounds. II. Synthesis and antihypertensive activity of mercaptoacylamino acids
Oya,Matsumoto,Takashina,Watanabe,Iwao
, p. 940 - 947 (2007/10/02)
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Version: 1.0
Creation Date: Aug 18, 2017
Revision Date: Aug 18, 2017
Product name | Bucillamine |
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Product number | - |
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Other names | (2R)-2-[(2-methyl-2-sulfanylpropanoyl)amino]-3-sulfanylpropanoic acid |
Identified uses | For industry use only. |
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Uses advised against | no data available |
Emergency phone number | - |
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Service hours | Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours). |
More Details:65002-17-7 SDS
S-benzyl-N-(S-benzyl-2-mercapto-2-methylpropanoyl)-L-cysteine
bucillamine
Conditions | Yield |
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With ammonia; sodium | 81% |
Conditions | Yield |
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With potassium carbonate; dicyclohexyl-carbodiimide 1.) EtOAc, r.t., 1 h; 2.) EtOAc, MeOH, water, r.t., 4 h; Yield given. Multistep reaction; |
bucillamine
methyl iodide
2-methylmercapto-isobutyroyl-l-S-methylcysteine
Conditions | Yield |
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With potassium carbonate for 1h; Ambient temperature; | 75% |
bucillamine
S-methyl-N-<2-methyl-2-(methylthio)propanoyl>-L-cysteine methyl ester
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 75 percent / 2 N potassium carbonate / 1 h / Ambient temperature 2: diethyl ether View Scheme |
diazomethane
bucillamine
N-(2-Mercapto-2-Methylpropionyl)-L-Cysteine Methyl Ester
Conditions | Yield |
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With acetic acid | 1.0 g(94%) |
trityl chloride
bucillamine
N-(2-Mercapto-2-Methylpropionyl)-S-Trityl-L-Cysteine
Conditions | Yield |
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In N-methyl-acetamide | 14.2 g(60%) |
bucillamine
(4R)-tetrahydro-7,7-dimethyl-6-oxo-3H-1,2,5-dithiazepine-4-carboxylic acid
Conditions | Yield |
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0.45 g (45%) |
bucillamine
S,S'-dinitrosobucillamine
Conditions | Yield |
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With sodium nitrite Acidic conditions; |
bucillamine
Conditions | Yield |
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at 20℃; |
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