653605-06-2

Basic information

• Product Name: 8,8'-DICHLORO-5,11,5',11'-TETRAMETHYL-5,6,11,12,5',6',11',12'-OCTAHYDRO-[2,2']BI[DIBENZO[B,F][1,5]DIAZOCINYL]
• Synonyms: 8,8'-DICHLORO-5,11,5',11'-TETRAMETHYL-5,6,11,12,5',6',11',12'-OCTAHYDRO-[2,2']BI[DIBENZO[B,F][1,5]DIAZOCINYL]
• CAS NO: 653605-06-2
• Molecular Formula: C32H32Cl2N4
• Molecular Weight: 543.53
• Mol File: 653605-06-2.mol
• Article Data: 1

Chemical Properties

• Appearance: /
• CAS DataBase Reference: 8,8'-DICHLORO-5,11,5',11'-TETRAMETHYL-5,6,11,12,5',6',11',12'-OCTAHYDRO-[2,2']BI[DIBENZO[B,F][1,5]DIAZOCINYL](CAS DataBase Reference)
• NIST Chemistry Reference: 8,8'-DICHLORO-5,11,5',11'-TETRAMETHYL-5,6,11,12,5',6',11',12'-OCTAHYDRO-[2,2']BI[DIBENZO[B,F][1,5]DIAZOCINYL](653605-06-2)
• EPA Substance Registry System: 8,8'-DICHLORO-5,11,5',11'-TETRAMETHYL-5,6,11,12,5',6',11',12'-OCTAHYDRO-[2,2']BI[DIBENZO[B,F][1,5]DIAZOCINYL](653605-06-2)

Safety Data

• Hazardous Substances Data: 653605-06-2(Hazardous Substances Data)

Upstream product

• 26772-93-0 N-(4-chlorophenyl)-N-methylformamide 
• 366-29-0 N,N,N',N'-tetramethylbenzidine 

Relevant articles and documents

A Simple One-Pot Reaction to the Bis-dibenzo[b,f][1,5]diazocines: Useful Precursors of Novel Macrocycles

The title compounds, namely 8,8′-bis-5,6,11,12-tetrahydrodibenzo[b,f] [1,5]diazocines, have been synthesized in 36-81% yields through a one-pot reaction by treatment of N,N,N′,N′-tetramethylbiphenyldiamine with the Vilsmeier's reagents derived from substituted N-methylformanilides and POCl3. This was another application of 't-amino effect' in the synthesis of eight-membered ring systems. These products are designed as the precursors of novel macrocycles.