677717-51-0

Basic information

• Product Name: 2',4'-dimethoxy[1-13C]acetophenone
• Synonyms: 2',4'-dimethoxy[1-13C]acetophenone
• CAS NO: 677717-51-0
• Molecular Weight: 181.192
• Mol File: 677717-51-0.mol
• Article Data: 1

Chemical Properties

• CAS DataBase Reference: 2',4'-dimethoxy[1-13C]acetophenone(CAS DataBase Reference)
• NIST Chemistry Reference: 2',4'-dimethoxy[1-13C]acetophenone(677717-51-0)
• EPA Substance Registry System: 2',4'-dimethoxy[1-13C]acetophenone(677717-51-0)

Safety Data

• Hazardous Substances Data: 677717-51-0(Hazardous Substances Data)

Upstream product

• 1520-57-6 [1-13C]acetyl chloride 
• 151-10-0 1,3-Dimethoxybenzene 

Downstream Products

• 677717-56-5 methyl 2,3-bis(2,4-dimethoxyphenyl)-3-[1,2,3-13C₃]oxopropanoate 
• 677717-54-3 2,4-dimethoxy[carboxy-13C]benzoyl chloride 
• 677717-53-2 [13C-carboxyl]-2,4-dimethoxybenzoic acid 

Relevant articles and documents

A new short synthesis of coumestrol and its application for the synthesis of [6,6a,11a-13C3]coumestrol

A convenient and simple two-step method for the synthesis of coumestrol has been established, which involves a base catalysed condensation of phenyl acetate with benzoyl chloride, followed by demethylation and subsequent tandem intramolecular cyclisation. This method was then employed for the efficient synthesis of multiply 13C-labelled coumestrol.