67874-69-5Relevant articles and documents
Synthesis of geranyl N-dimethylallylanthranilate, a new antimicrobial natural product from Esenbeckia yaaxhokob
Sharma,Sharma,Rathee, Raman
, p. 1158 - 1159 (2008/02/07)
A convenient synthesis of geranyl N-dimethylallylanthranilate 1, utilizing DMAP mediated esterification of isatoic anhydride 2 with geraniol 3 and subsequent N′-alkylation of the resulting ester 4 using tetrabutylammonium iodide with 3,3-dimethylallyl bromide 5 has been achieved in 88.2% yield. The identity with the naturally occurring compound was established on the basis of 1H NMR and 13C NMR data.