68521-59-5Relevant academic research and scientific papers
α-Thiocyanation of Ketones and Esters Using (Dichloroiodo)benzene-Lead(II) Thiocyanate
Prakash, Om,Rani, Neena,Sharma, Vijay,Moriarty, Robert M.
, p. 1255 - 1256 (1997)
Reaction of enol silyl ethers of acetophenone, 2-acetylfuran, 2-acetylthiophene, 2-acetylpyridine, cyclopentanone and cyclohexanone, and ketene silyl acetals of arylacetic esters with a combination of lead(II) thiocyanate and (dichloroiodo)benzene affords
α-thiocyanation of carbonyl and β-dicarbonyl compounds using (dichloroiodo)benzene-lead(II) thiocyanate
Prakash,Kaur,Batra,Rani,Singh,Moriarty
, p. 2019 - 2023 (2007/10/03)
The combination reagent (dichloroiodo)benzene and lead(II) thiocyanate in dichloromethane effects oxidation of various enol silyl ethers, ketene silyl acetals, and β-dicarbonyl compounds, thereby providing an efficient and convenient method for α-thiocyanation of carbonyl and β-dicarbonyl compounds.
