72637-18-4Relevant articles and documents
Refining and purification method and drying treatment apparatus for 2-chloronicotinic acid
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Paragraph 0027; 0029; 0034; 0038; 0040; 0045; 0049; 0051, (2019/10/01)
The invention discloses a refining and purification method and a drying treatment apparatus for 2-chloronicotinic acid. The method comprises the following steps: reacting 3-methylpyridine with chlorine to produce 2-chloro-3-trichloromethylpyridine; hydrolyzing 2-chloro-3-trichloromethylpyridine to obtain a 2-chloronicotinic acid reaction product; and purifying and drying the 2-chloronicotinic acidreaction product by using the apparatus. The apparatus is applicable to drying treatment of 2-chloronicotinic acid and has a simple structure. The refining and purification method for 2-chloronicotinic acid can greatly improve the quality and purity of a 2-chloronicotinic acid product.