73340-33-7Relevant articles and documents
Method for preparing 2, 2-bis (3-nitro-4-hydroxyphenyl) hexafluoropropane by microchannel reactor
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Paragraph 0029-0046, (2021/07/14)
The invention discloses a method for preparing 2, 2-bis (3-nitro-4-hydroxyphenyl) hexafluoropropane by a microchannel reactor. The method comprises the following steps: (1) fully mixing and preheating bisphenol AF and an organic solvent to obtain a bisphenol AF solution, and respectively introducing the bisphenol AF solution and a preheated nitrating agent as two strands of materials into a continuous flow microchannel reactor through a metering pump; (2) controlling the flow rate of the material through a metering pump, enabling the bisphenol AF solution and the nitrating agent to respectively enter a micro-channel reactor module for mixed reaction, and enabling a product to flow out from an outlet of the reactor; and (3) carrying out post-treatment on the material obtained from the outlet of the microchannel reactor to obtain a pure product of 2, 2-bis (3-nitro-4-hydroxyphenyl) hexafluoropropane. The method provided by the invention can realize continuous production, has mild reaction conditions, high reaction efficiency and high yield, and is suitable for industrial production.
Preparation method for bis(3-amino-4-hydroxyphenyl)hexafluoropropane
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Paragraph 0110-0115, (2020/07/13)
The invention belongs to the technical field of electronic chemical materials, and more specifically relates to a preparation method for bis(3-amino-4-hydroxyphenyl)hexafluoropropane. The preparationmethod for the bis(3-amino-4-hydroxyphenyl)hexafluoropropane disclosed by the invention comprises the following steps: step 1, introducing hexafluoroacetone into a reactant (I) in the presence of a catalyst for a reaction so as to obtain a compound (II); step 2, allowing the compound (II) obtained in the step 1 with nitric acid and sulfuric acid so as to obtain a compound (III); step 3, adding thecompound (III) obtained in the step 2 into inorganic base for a reaction so as to obtain a compound (IV); and step 4, carrying out catalytic hydrogenation on the compound (IV) obtained in the step 3so as to obtain the bis(3-amino-4-hydroxyphenyl)hexafluoropropane.
Method of producing 2,2-bis(3-nitro-4-hydroxyphenyl)hexafluoropropane
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, (2008/06/13)
Disclosed herein is a method of producing 2,2-bis(3-nitro-4-hydroxphenyl)hexafluoropropane, which comprises (a) preparing 2,2-bis(4-hydroxyphenyl)hexafluoropropane and a lower fatty acid; and (b) allowing the 2,2-bis(4-hydroxyphenyl)hexafluoropropane to react with nitric acid in the lower fatty acid.