74629-69-9Relevant academic research and scientific papers
Catalyst-free synthesis of 2,3-dihydro-1,5-benzothiazepines in a renewable and biodegradable reaction medium
Yadav, Neetu,Yadav, Vijay B.,Ansari, Mohd Danish,Sagir, Hozeyfa,Verma, Ankit,Siddiqui
supporting information, p. 7011 - 7014 (2019/05/17)
A clean and efficient strategy for the synthesis of benzothiazepines from chalcone and ortho-aminothiophenol has been reported. Here, glycerol, a biodegradable and reusable promoting medium, has been utilized under acid, base or metal-free conditions. The
A practical synthesis of 2,3-dihydro-1,5-benzothiazepines
Albanese, Domenico C. M.,Gaggero, Nicoletta,Fei, Meng
supporting information, p. 5703 - 5707 (2017/12/06)
2,3-Dihydro-1,5-benzothiazepines have been obtained through a domino process involving a Michael addition of 2-aminothiophenols to chalcones, followed by in situ cyclization. Up to 98% chemical yields have been obtained at room temperature under essential
Solvent-free synthesis of 1,5-benzothiazepines and benzodiazepines on inorganic supports
Kodomari, Mitsuo,Noguchi, Tomohiro,Aoyama, Tadashi
, p. 1783 - 1790 (2007/10/03)
1,5-Benzothiazepines and 1,5-benzodiazepines have been synthesized in solvent-free conditions from chalcones and o-aminothiophenol or o-phenylenediamine in the presence of inorganic support. Silica gel was found to be an effective support for the synthesi
Synthesis of 2,4-diaryl-1,5-berizodiazepines and 2,4-diaryl-2,3-dihydro-1,5-benzothiazepines
Padwad, Manisha,Ingle
, p. 161 - 162 (2007/10/03)
Various 2,4-disubstituted-1,5-benzodiazepines have been prepared by condensing 1,3-diones with o-phcnylencdiaminc, and 2,4-diaryl 2,3-dihydro-1,5-benzothiazepines have been prepared by condensing hydroxychalconc and o-aminothiophenol in boiling dry xylene
Syntheses and Spectral Studies of Some 2-(Substituted phenyl)-4-phenyl-1,5-benzothiazepines
Gupta, A. K.,Singh, V. K.,Pant, Umesh C.
, p. 1057 - 1059 (2007/10/02)
2,3-Dihydro-2-(substituted phenyl)-4-phenyl-1,5-benzothiazepines (XI-XIX) have been synthesized in good yields by reacting chalkones (I-IX) with 2-aminobenzenethiol.The hydroxyl group at position 2 or 4 alone or along with other groups in ring-B has been
