7617-40-5Relevant academic research and scientific papers
STEREOSPECIFIC REDUCTION OF DIASTEREOMERICALLY PURE MENTHYL PHOSPHINATES: A NEW ROUTE TO OPTICALLY ACTIVE PHOSPHINE OXIDES
Koide, Yasuhiro,Sakamoto, Atsushi,Imamoto, Tsuneo
, p. 3375 - 3376 (2007/10/02)
Diastereomerically pure menthyl phosphinates are stereospecifically reduced by lithium 4,4'-di-tert-butylbiphenylide.Subsequent treatment with alkyl halides affords phosphine oxides with high optical purity.
DETERMINATION OF THE ABSOLUTE CONFIGURATIONS OF 1,2-DIPHOSPHINYLETHENES POSSESSING TWO NONEQUIVALENT ASYMMETRIC PHOSPHORUS CENTRES. CRYSTAL STRUCTURE OF (R,S)-1-(tert-BUTYLPHENYLPHOSPHINYL)-2-(METHYL-PHENYLPHOSPHINYL)ETHANE.
Pietrusiewicz, K. Michal,Zablocka,Maria,Wieczorek, Wanda
, p. 183 - 190 (2007/10/02)
Using signle-crystal X-ray diffraction technique the R,S configuration has been assigned to a homochiral (-)-1-tert-butylphenylphosphinyl-2-methhylphenylphosphinylethane.This has allowed the assignment of absolute configuration also to its P1-epimer as we
OPTICALLY ACTIVE PHOSPHINE OXIDES. 4. A STRAIGHTFORWARD SYNTHESIS OF P-CHIRAL 1,2-DIPHOSPHINOYLETHANES.
Pietrusiewicz, K. Michal,Zablocka, Maria
, p. 1987 - 1990 (2007/10/02)
The title compounds possesing either one or two homochiral phosphorus centres are conveniently prepared via non-catalyzed addition of secondary phosphine oxides to an optically active vinyl phosphine oxide.
