7749-48-6Relevant academic research and scientific papers
Synthesis of hitherto unknown 4,4-bis(Methylthio)but-3-en-2-one-1,1,1,3- d4 and its application as 1,3-dielectrophilic building block for the synthesis of deuterated heterocycles and aromatics
Charanraj,Ramachandra,Ramesh,Junjappa
, p. 412 - 417 (2018/05/22)
Acetone-d6 has been transformed for the first time to 4,4-bis(methylthio)but-3-en-2-one- 1,1,1,3-d4. This tetradeutero-α-oxoketenedithioacetal is shown to be an excellent 1,3-dielectrophilic building block for the synthesis of 5- and
Research on heterocyclic compounds - Part XXXIX. 2-Methylimidazo[1,2-a]pyrimidine-3-carboxylic derivatives: Synthesis and antiinflammatory activity
Laneri, Sonia,Sacchi, Antonia,Gallitelli, Marina,Arena, Francesca,Luraschi, Elena,Abignente, Enrico,Filippelli, Walter,Rossi, Francesco
, p. 163 - 170 (2007/10/03)
The synthesis of a group of 2-methylimidazo[1,2-a]pyrimidine-3-carboxylic esters, acids and amides is described. The structures of new compounds are supported by 1H and 13C NMR spectra. These compounds were tested in vivo for their antiinflammatory analgesic and ulcerogenic activity. Eight new compounds out of fifteen showed remarkable dose-dependent antiinflammatory action in die carrageenan rat paw edema (1/2-1/3 x indomethacin) but weak analgesic activity in the acetic acid writhing test together with negligible ulcerogenic action. The new compounds were found to be lacking in inhibitory activity on cyclooxygenase in vitro.
