78743-57-4Relevant articles and documents
A FACILE SYNTHESIS OF 1,3-CYCLOALKADIONES
Nishiguchi, Ikuzo,Hirashima, Tsuneaki,Shono, Tatsuya,Sasaki, Manji
, p. 551 - 554 (2007/10/02)
1,3-Cycloalkadiones were prepared by the reaction of 1,2-bis(trimethylsiloxy)cycloalkenes with chloromethyl methyl ether followed by treatment of the resulting 2-hydroxy-2-methoxymethyl cycloalkanones with potassium hydrogen sulfate.The first step of the reactions was effectively catalyzed by active zinc reagents prepared from zinc-copper and alkyl iodides.