86116-17-8Relevant articles and documents
One-pot synthesis of thioesters with sodium thiosulfate as a sulfur surrogate under transition metal-free conditions
Liao, Yen-Sen,Liang, Chien-Fu
, p. 1871 - 1881 (2018/03/23)
In this paper, we report an efficient synthetic method for thioester formation from sodium thiosulfate pentahydrate, organic halides, and aryl anhydrides. In the one-pot two-step reactions developed in this study, sodium thiosulfate was used as the sulfur surrogate for acylation with anhydrides, followed by substitution with organic halides through the in situ generation of thioaroylate. Furthermore, two important organic compounds could be successfully synthesized using our developed method. The advantages of the one-pot two-step reactions are operational simplicity, structurally diverse products with 42%-90% yields, use of relatively low toxic and odourless reagents, and easy applicability to large-scale operation.
An odorless, one-pot synthesis of thioesters from organic halides, thiourea and benzoyl chlorides in water
Lu, Guo-Ping,Cai, Chun
supporting information, p. 1271 - 1276 (2013/06/26)
Thioesterification can be realized via an odorless, one-pot reaction through the in situ generation of S-alkylisothiouronium salts from organic halides and thiourea in aqueous Triton X-100 (TX100) micelles. The protocol is free of foul-smell thiols and or
CHOLYNOLITIC ACTIVITY OF PIPERIDINOBUTINE ESTERS OF CERTAIN CARBOXYLIC ACIDS
Starshinova, L. A.,Shelkonikov, S. A.,Vikhreva, L. A.,Pudova, T. A.,Gulyamov, M.,et al.
, p. 818 - 821 (2007/10/02)
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