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Studies on Organophosphorus Compounds. XXXIV. Syntheses of 2,3-Dihydro-1,3,4,2-Thiadiazaphospholes and Thiohydrazides
El-Barbary, A. A.,Scheibye, S.,Lawesson, S.-O.,Fritz, H.
, p. 597 - 602 (2007/10/02)
N'-Substituted hydrazides, 2, react with 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide, 1, in refluxing benzene to give 2,3-dihydro-1,3,4,2-thiadizaphospholes, 3; in one case also the thiohydrazide, 4e, was isolated.Benzohydrazide, 10
