86934-59-0Relevant articles and documents
Phosphinoalkylsilanes: Synthesis and Spectroscopic Properties of Phosphino(sylil)methanes, 1-Phosphino-2-silylethanes, and 1-Phosphino-3-silylpropanes
Holmes-Smith, Rupert D.,Osei, Rexford D.,Stobart, Stephen R.
, p. 861 - 866 (2007/10/02)
Synthesis of thirty-three compounds Ph2P(CH2)nSiXYZ (n=1, 2, or 3) and Me2P(CH2)2SiXYZ in which X, Y, or Z=H, Me, Ph, or Cl has been accomplished by (a) reaction at -78 deg C in tetrahydrofuran between alkyl(chloro)silanes and Ph2PCH2Li*tmeda for n = !, o