86967-50-2Relevant academic research and scientific papers
Efficient Synthesis of N-Triphenylmethyl α-Amino Acids
Mutter, Manfred,Hersperger, Rene
, p. 198 - 200 (2007/10/02)
A new one-pot synthesis of N-triphenylmethyl(trityl) α-amino acids 3 via their trityl ester 2 has been developed.
PREAPARATION OF TRITYL DERIVATIVES OF AMINO ACIDS WITH THE AID OF THE SILYLATION REACTION
Rabinovich, A. K.,Karelskii, V. N.,Krysin. E. P.,Antonov, A. A.,Smirnov, M. B.,Chipens, G. I.
, p. 205 - 207 (2007/10/02)
A number of N-trityl-substituted amino acids (lysine, glutamine, tyrosine, valine, and proline) have been obtained with the aid of the silylation reaction.Bis(trimethylsilyl)acetamide was used as the silylating agent.The compounds were isolated with good yields and were distinguished by chromatographic homogeneity, and they were characterized by their angles of optical rotation, melting points, and elementary analyses.Their purity was checked by TLC and 13C NMR.
