915777-70-7

Basic information

• Product Name: 1H-2-Benzazepine-4-carboxylic acid, 2,3-dihydro-3-phenyl-2-[[2-(trimethylsilyl)ethyl]sulfonyl]-, methyl ester
• CAS NO: 915777-70-7
• Molecular Formula: C23H29NO4SSi
• Molecular Weight: 443.639
• Mol File: 915777-70-7.mol
• Article Data: 2

Chemical Properties

• CAS DataBase Reference: 1H-2-Benzazepine-4-carboxylic acid, 2,3-dihydro-3-phenyl-2-[[2-(trimethylsilyl)ethyl]sulfonyl]-, methyl ester(CAS DataBase Reference)
• NIST Chemistry Reference: 1H-2-Benzazepine-4-carboxylic acid, 2,3-dihydro-3-phenyl-2-[[2-(trimethylsilyl)ethyl]sulfonyl]-, methyl ester(915777-70-7)
• EPA Substance Registry System: 1H-2-Benzazepine-4-carboxylic acid, 2,3-dihydro-3-phenyl-2-[[2-(trimethylsilyl)ethyl]sulfonyl]-, methyl ester(915777-70-7)

Safety Data

• Hazardous Substances Data: 915777-70-7(Hazardous Substances Data)

Upstream product

• 100-52-7 benzaldehyde 
• 125486-96-6 2-(trimethylsilyl)ethanesulfonamide 
• 816457-61-1 methyl 2-(phenyl(2-(trimethylsilyl)ethylsulfonamido)methyl)acrylate 
• 915777-58-1 methyl 2-((N-2-bromobenzyl-2-(trimethylsilyl)ethan-3-ylsulfonamido)(phenyl)methyl)acrylate 
• 3433-80-5 1-Bromo-2-bromomethyl-benzene 

Relevant articles and documents

A microwave-assisted heck reaction in poly(ethylene glycol) for the synthesis of benzazepines

The Heck reaction of alkylated 2-(trimethylsilyl)ethanesulfonyl (SES)-protected β-amino esters provides benzazepines in good yields. Good selectivity towards cyclisation was obtained when the reaction was performed in PEG 3400 as the solvent under microwa