915777-72-9Relevant articles and documents
A microwave-assisted heck reaction in poly(ethylene glycol) for the synthesis of benzazepines
Declerck, Valerie,Ribiere, Patrice,Nedellec, Yannig,Allouchi, Hassan,Martinez, Jean,Lamaty, Frederic
, p. 201 - 208 (2007/10/03)
The Heck reaction of alkylated 2-(trimethylsilyl)ethanesulfonyl (SES)-protected β-amino esters provides benzazepines in good yields. Good selectivity towards cyclisation was obtained when the reaction was performed in PEG 3400 as the solvent under microwa