92252-86-3Relevant articles and documents
Chemoselective synthesis of 1,1-diacetates from aldehydes using anhydrous cobalt(II) bromide under solvent-free conditions
Meshram, Gangadhar A.,Patil, Vishvanath D.
, p. 442 - 449 (2010)
A mild and efficient method has been developed for the chemoselective preparation of 1,1-diacetates (acylals) from aldehydes catalyzed in the presence of a catalytic amount (0.1mmol) of anhydrous cobalt(II) bromide under solvent-free conditions. The remarkable selectivity under mild and neutral conditions, excellent yields, short reaction time, and easily available and inexpensive catalyst are important features of this method.
Synthesis and Reactions of 1,3-Benzodioxoledicarboxaldehydes. A Contribution to the Structure Elucidation of Nepenthone-A
Dallacker, Franz,Schleuter, Hans-Joachim,Schneider, Petra
, p. 1273 - 1280 (2007/10/02)
We describe the preparation of 1,3-Benzodioxole-5,6-dicarboxaldehyde (1d) and 1,3-Benzodioxole-4,5-dicarboxaldehyde (3h).Under especially mild conditions also the synthesis of 4,7-Dimethoxy-1,3-benzodioxole-5,6-dicarboxaldehyde (4g) can be achieved.Its re