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2,6-Dichlorodiphenylamine
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Name

2,6-Dichlorodiphenylamine

 EINECS 239-349-0
CAS No. 15307-93-4 Density 1.327 g/cm3
PSA 12.03000 LogP 4.81000
Solubility N/A Melting Point 50-53 °C(lit.)
Formula C12H9Cl2N Boiling Point 309.795 °C at 760 mmHg
Molecular Weight 238.116 Flash Point 141.159 °C
Transport Information N/A Appearance Off white to cream coloured Crystalline solid
Safety 26-36 Risk Codes 36/37/38
Molecular Structure Molecular Structure of 15307-93-4 (2,6-DICHLORODIPHENYLAMINE) Hazard Symbols IrritantXi
Synonyms

Diphenylamine,2,6-dichloro- (8CI);2,6-Dichlorodiphenylamine;N-(2,6-Dichlorophenyl)aniline;N-Phenyl-2,6-dichloroaniline;

Article Data 14

2,6-Dichlorodiphenylamine Synthetic route

108-90-7

chlorobenzene

608-31-1

2,6-Dichloroaniline

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With copper(II) oxide In 1,4-dioxane at 130℃; for 20h; Reagent/catalyst; Solvent;95%
108-86-1

bromobenzene

608-31-1

2,6-Dichloroaniline

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With johnphos; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) In toluene for 1h; Heating;94%
146607-19-4

2-(2,6-dichlorophenoxy)-N-phenylacetamide

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With sodium hydroxide In water; toluene at 80 - 90℃; for 4h; Reagent/catalyst; Temperature;93%
87-65-0

2,6-Dichlorophenol

527-60-6

Mesitol

7462-76-2

2-chloro-2-phenylacetamide

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With sodium hydroxide In water; N,N-dimethyl-formamide; toluene90.75%
123066-65-9

N-phenyl-2,2,6,6-tetrachlorocyclohexaneimine

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With sodium hydroxide In chlorobenzene85%
With triethylamine In N,N-dimethyl-formamide at 95 - 100℃; for 5h; Dehydrochlorination;
19393-92-1

1-bromo-2,6-dichlorobenzene

62-53-3

aniline

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With potassium phosphate; DavePhos; tris-(dibenzylideneacetone)dipalladium(0)
Stage #1: 1-bromo-2,6-dichlorobenzene; aniline With sodium t-butanolate In toluene for 0.5h; Inert atmosphere;
Stage #2: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In toluene for 18h; Reflux;
3776-30-5

2,2,6,6-tetrachlorocyclohexanone

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C
2: Et3N / dimethylformamide / 5 h / 95 - 100 °C
View Scheme
62-53-3

aniline

Wang resin-bound styrene 4

Wang resin-bound styrene 4

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C
2: Et3N / dimethylformamide / 5 h / 95 - 100 °C
View Scheme

C15H13Cl2NO2

15307-93-4

N-phenyl-2,6-dichloroaniline

Conditions
ConditionsYield
With potassium hydroxide at 130℃; for 2h;138 mg
15307-79-6

diclofenac sodium

A

59-48-3

2-oxoindole

B

87-65-0

2,6-Dichlorophenol

C

15362-40-0

1-(2,6-dichlorophenyl)indolin-2-one

D

69220-40-2

4-chloro-10(H)acridin-9-one

E

601-88-7

2,6-dichloronitrobenzene

F

15307-93-4

N-phenyl-2,6-dichloroaniline

G

10113-35-6

N-(2,6-dichlorophenyl)-formamide

H

6697-95-6

1,3-dichloro-2-isocyanobenzene

I

39920-37-1

2,6-dichlorophenylisocyanate

J

13603-93-5

4-chloro-1,3-benzoxazol-2(3H)-one

K

608-31-1

2,6-Dichloroaniline

Conditions
ConditionsYield
With dihydrogen peroxide; iron(II) In water at 20℃; pH=2; Fenton Reaction;
...Expand

2,6-Dichlorodiphenylamine Specification

The Benzenamine,2,6-dichloro-N-phenyl- is an organic compound with the formula C12H9Cl2N. The IUPAC name of this chemical is 2,6-Dichloro-N-phenylaniline. With the CAS registry number 15307-93-4, it is also named as (2,6-Dichlorophenyl)phenylamine. The product's categories are Anilines, Aromatic Amines and Nitro Compounds. Besides, its molecular weight is 238.11.

Physical properties about Benzenamine,2,6-dichloro-N-phenyl- are: (1)ACD/LogP: 4.77; (2)ACD/LogD (pH 5.5): 4.77; (3)ACD/LogD (pH 7.4): 4.77; (4)ACD/BCF (pH 5.5): 2492.27; (5)ACD/BCF (pH 7.4): 2492.27; (6)ACD/KOC (pH 5.5): 9394.62; (7)ACD/KOC (pH 7.4): 9394.62; (8)#H bond acceptors: 1; (9)#H bond donors: 1; (10)#Freely Rotating Bonds: 2; (11)Polar Surface Area: 3.24 Å2; (12)Index of Refraction: 1.649; (13)Molar Refractivity: 65.41 cm3; (14)Molar Volume: 179.3 cm3; (15)Polarizability: 25.93×10-24 cm3; (16)Surface Tension: 48 dyne/cm; (17)Density: 1.327 g/cm3; (18)Flash Point: 141.2 °C; (19)Enthalpy of Vaporization: 55.06 kJ/mol; (20)Boiling Point: 309.8 °C at 760 mmHg; (21)Vapour Pressure: 0.000625 mmHg at 25 °C. 

Uses of Benzenamine,2,6-dichloro-N-phenyl-: it can be used to produce 2-Chloro-N-(2',6'-dichlorophenyl)-N-phenylacetamide. The reaction time is 16 hours. The yield is about 66%.

When you are using this chemical, please be cautious about it as the following:
It is irritating to eyes, respiratory system and skin. When you are using it, wear suitable protective clothing. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.

You can still convert the following datas into molecular structure:
(1)InChI: InChI=1/C12H9Cl2N/c13-10-7-4-8-11(14)12(10)15-9-5-2-1-3-6-9/h1-8,15H
(2)InChIKey: HDUUZPLYVVQTKN-UHFFFAOYAC
(3)Std. InChI: InChI=1S/C12H9Cl2N/c13-10-7-4-8-11(14)12(10)15-9-5-2-1-3-6-9/h1-8,15H
(4)Std. InChIKey: HDUUZPLYVVQTKN-UHFFFAOYSA-N

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