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110590-84-6

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Basic Information
CAS No.: 110590-84-6
Name: N,N'-BIS(1-HEXYLHEPTYL)-PERYLENE-3,4:9,10-BIS-(DICARBOXIMIDE)
Article Data: 30
Molecular Structure:
Molecular Structure of 110590-84-6 (N,N'-BIS(1-HEXYLHEPTYL)-PERYLENE-3,4:9,10-BIS-(DICARBOXIMIDE))
Formula: C50H62 N2 O4
Molecular Weight: 755.053
Synonyms: 2,9-Bis(1-hexyl-hept-1-yl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetrone;BHPD; N,N'-Bis(1-hexylheptyl)-3,4:9,10-perylenebis(dicarboximide);N,N'-Bis(1-hexylheptyl)-3,4:9,10-perylenetetracarboxylic diimide;N,N'-Bis(1-hexylheptyl)perylene-3,4:9:10-tetracarboxylic bisimide
Density: 1.149±0.06 g/cm3(Predicted)
Melting Point: 157-158 °C(Solv: methanol (67-56-1))
Boiling Point: 842.4±38.0 °C(Predicted)
Safety:
WGK Germany 3
PSA: 78.14000
LogP: 12.92680
Related products
Synthetic route
22513-16-2

1-hexylheptylamine

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
With 1H-imidazole at 180℃; for 5h;100%
With 1H-imidazole In dichloromethane at 150℃; for 5h;100%
With 1H-imidazole; zinc diacetate at 155℃; for 4h;99%
288-32-4

1H-imidazole

22513-16-2

1-hexylheptylamine

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

9-(1-hexylheptyl)-2-[1-hexyl-2-(1H-imidazol-1-yl)heptyl]anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetrone

B

2,9-bis[1-hexyl-2-(1H-imidazol-1-yl)heptyl]anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetrone

C

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
at 160℃; for 4h;A 0.7%
B 0.07%
C 82%
...Expand

C40H43NO6

106-94-5

propyl bromide

A

1274451-95-4

N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide

B

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 25℃; for 16h;A 58%
B 15%
...Expand
22513-16-2

1-hexylheptylamine

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

198-55-0

PERYLENE

B

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

C

165261-27-8

2-(1-hexylheptyl)-1H-benzo-[5,10]anthra[2,1,9-def ]isoquinolin-1,3(2H)-dione

Conditions
ConditionsYield
With 1H-imidazole; zinc diacetate; water at 190℃; for 24h;A n/a
B 15%
C 27%
...Expand
462-18-0

tridecan-7-one

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / NH4OAc; NaBH3CN / methanol / 48 h / 20 °C
2: imidazole / 5 h / 180 °C
View Scheme
Multi-step reaction with 2 steps
1: ammonium acetate; sodium cyanoborohydride / methanol / 56 h / 20 °C
2: 1H-imidazole / 3 h / 130 °C
View Scheme
Multi-step reaction with 2 steps
1: ammonium acetate; sodium cyanoborohydride / methanol / 60 h / 20 °C
2: 1H-imidazole / 4 h / 160 °C
View Scheme
26077-63-4

tridecan-7-one oxime

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium-dihydrobis(2-methoxyethoxy)aluminate / toluene / 4 h / 140 °C
2: 41 percent / imidazole / 4 h / 160 °C
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran
2: 1H-imidazole / 150 °C
View Scheme
22513-16-2

1-hexylheptylamine

138536-82-0

4-(5,5-dimethyl-1,3-dioxan-2-yl)benzylamine

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

C50H52N2O6

B

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
With 1H-imidazole at 160℃; for 24h;
...Expand
22513-16-2

1-hexylheptylamine

A

1274451-95-4

N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide

B

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 16 h / 25 °C
1.2: 72 h / 25 °C
2.1: N,N-dimethyl-formamide / 16 h / 25 °C
View Scheme
128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

A

1274451-95-4

N-(1-hexylheptyl)-9,10-bis(propyloxycarbonyl)perylene-3,4-dicarboximide

B

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 16 h / 25 °C
1.2: 72 h / 25 °C
2.1: N,N-dimethyl-formamide / 16 h / 25 °C
View Scheme
462-18-0

tridecan-7-one

128-69-8

perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

110590-84-6

N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide

Conditions
ConditionsYield
Stage #1: tridecan-7-one With ammonium acetate; sodium cyanoborohydride In methanol at 20℃; for 48h; Inert atmosphere;
Stage #2: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With 1H-imidazole at 130℃; for 3h; Inert atmosphere;		8.57 g
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